ISOLASI KUMARIN DARI KULIT BUAH LIMAU SUNDAI (Citrus nobilis Lour)

Authors

  • Melindra Mulia Jurusan Kimia Universitas Negeri Padang

DOI:

https://doi.org/10.24036/eksakta/vol18-iss02/70

Keywords:

Citrus nobilis Lour, coumarin, isolation, characteritation, marmin

Abstract

Coumarin has been isolated and characteritated from rind of  Citrus nobilis Lour by maseration methode with methanol. After fractionation by n-hexane and ethyl acetate, collected the phase ethyl acetate which positive of coumarin. From ethyl acetate extract coumarin have been isolated by column chromatography. The isolation results was obtain 2,159 g of pure white needle-shape crystalline with the melting point of 126,2-127,60C. Structure of the isolated coumarine was elucidated by spectroscopic methodes, UV-Vis,13C-NMR, 1H-NMR, 2D-NMR (DEPT/HSQC, COSY, NOESY, HMBC) and IR spectra. Based on the spectra data the isolated coumarine is marmin.

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Published

2017-11-30

Issue

Vol. 18 No. 02 (2017): Eksakta : Berkala Ilmiah Bidang MIPA (E-ISSN : 2549-7464)

Section

EKSAKTA: Berkala Ilmiah Bidang MIPA

License

This is an open-access article distributed under the terms of the Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License (http://creativecommons.org/licenses/by/4.0/) which permits unrestricted non-commercial use, distribution and reproduction in any medium

How to Cite

1.
ISOLASI KUMARIN DARI KULIT BUAH LIMAU SUNDAI (Citrus nobilis Lour). EKSAKTA [Internet]. 2017 Nov. 30 [cited 2026 Aug. 2];18(02):137-45. Available from: https://eksakta.ppj.unp.ac.id/index.php/eksakta/article/view/70

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