Article Sidebar

Submitted
Sep 12, 2020
Accepted
Sep 27, 2020
Published
Sep 30, 2020
Download
pdf
Statistic
Read Counter : 699 Download : 535

Downloads

Download data is not yet available.

Main Article Content

Abstract

This research aims to study the production of essential oil from Piper Cubeba using the solvent-free microwave extraction (SFME) method. Before extraction, the raw materials are prepared in the form of grains and powders to vary the size of the raw materials. Time variation was carried out at microwave power 180 Watt Analyses were then performed on the resulting essential oil using both physical and chemical tests of density and solubility with 96% alcohol. Analyses of chemical compounds within the essential oil were then performed using the Gas Chromatograph Mass Spectrometry (GC-MS). It was found that the production of essential oil from Piper Cubeba using the SFME method was affected by microwave power, grain size, and treatment duration. Results from physical and chemical analyses revealed that the resulting cubeb oil has 0.86 g/mL density, which means that essential oil produced using the SFME method is lighter compared than those produced using MAHD methods. Results from GC-MS analyses showed eight components detected from the production of essential oil from Piper cubeba using the SFMEmethod; Copaene (39.28%), Cubebene (23.83%), Isoledene (11.66%), Naphthalene (6.65%), Phellandrene (5.81%), Asarone (5.71%), Cadidene (4.90%), and Caryophyllene (2.16%) which contents belong to the sesquiterpene group

Keywords

Extraction, Essential oil, Piper cubeba, SFME, Time , Grain size

Article Details

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

How to Cite
1.
Eralita N, Khuzaimah S. The Extraction of Essential Oil from Piper Cubeba by Using Solvent Free Microwave Extraction Method. EKSAKTA [Internet]. 2020Sep.30 [cited 2024Apr.19];21(2):85-97. Available from: https://eksakta.ppj.unp.ac.id/index.php/eksakta/article/view/239

References

  1. Rahmi, D. (2018) "Balai Besar Kimia dan Kemasan," Balai Besar Kimia dan Kemasan, 17 April 2018. [Online].available:http://bbkk.kemenperin.go.id/page/ bacaartikel.php?id= OSCDT-7v3kbO42NmtwHDAEGAxVG96ARtA072jn2iwylQ,. [Accessed 26 Agustus 2019].
  2. Supomo,S., Warnida,H and Said, BM.(2019) Perbandingan Metode Ekstraksi Umbi Bawang Rambut (Allium chinense G, Don) Menggunakan Pelarut Etanol 70% Terhadap Rendemen dan Skrining FitoKimia. Jurnal Riset Kefarmasian Indonesia. 1 (1), 30-40
  3. Resno, M., Sudaryat,Y and Widyastiw.(2019). Aktivitas Immunodilator Ekstrak Etanol Kemukus (Piper cubeba), Kiseureuh (Piper aduncum), dan Cabe Jawa (Piper rertofactum) pada Mencit Jantan Galur Balb/C. Jurnal Ilmu Kefarmasian Indonesia. 17(2), 255-261
  4. Susanty, Y.(2007). Pembuatan Permen Tablet Pastiles dengan Bahan Aktif Minyak Kemukus (Pipper cubeba linn). Institut Pertanian Bogor, Bogor.
  5. Susanty, Y.(2007) Pembuatan Permen Tablet Pastiles dengan Bahan Aktif Minyak Kemukus (Pipper cubeba linn). Institut Pertanian Bogor, Bogor.
  6. Triyana, A.W.(2013). Ekstraksi Minyak Atisri Biji Kemukus Dengan Metode Microwave-Assisted Hydro Distillation. Universitas Padjajaran, Semarang: Fakultas Teknik.
  7. Lucchesi, M.E; Chemat, F; Smadja, J .(2016). Solvent-Free Microwave Extraction: An Innovative Tool for Rapid Extraction of Essential Oil From Aromatic Herbs and Spices. Journal of Microwave Power & electromagnetic Energy. 39(10), 3-4.
  8. Sulaswatty, A.(2003). Pemurnian Minyak Nilam (Pogostemon cablin benth) Menggunakan Teknik Ekstraksi Superkritik. pusat Percobaan Kimia Lembaga Ilmu Pengetahuan Indonesia (LIPI), Tengerang.
  9. Ashgari, J.(2011). Microwave-Assisted Hydro Distillation of Essential Oils from Echinophora platyloba DC. Journal of Medicinal Plants Research, 6(28), 4475-4480.
  10. Okoh, O.(2011). Antioxidant Activities of Rosmarinus officinalis L., Essential Oil Obtained by Hydro Distillation and Solvent Free Microwave Extractioan. African Journal of Biotechnology . 10(20), 4207-4211.
  11. Sulaswatty, A.(2003). Pemurnian Minyak Nilam (Pogostemon cablin benth) Menggunakan Teknik Ekstraksi Superkritik. pusat Percobaan Kimia Lembaga Ilmu Pengetahuan Indonesia (LIPI). Tengerang.
  12. Wang, J.(2008). Study of Vacuum Microwave-Assisted Extraction of Polyphenol Compounds and Pigment from Chinese Herbs. Journal of Chromatography, 1(198), 45-53.
  13. J Ashgari, J.(2011). Microwave-Assisted Hydro Distillation of Essential Oils from Echinophora platyloba DC. Journal of Medicinal Plants Research, 6(28), 4475-4480.
  14. Chen.(2011). Optimization of Solvent-Free Microwave Extraction of Essential Oil from the Fruits of Schidndra chinenses and its DPPH Radical Scavenging Activity. Food Science, 32(14), 85-89.
  15. Lucchesi, M.E; Chemat, F; Smadja, J. (2016). Solvent-Free Microwave Extraction: An Innovative Tool for Rapid Extraction of Essential Oil From Aromatic Herbs and Spices. Journal of Microwave Power & electromagnetic Energy , 39(10), 3-4.
  16. Ruwindya, Y. (2019). Optimasi Metode Analisis Minyak Atsiri Sereh Wangi Secara Kromatografi Gas. Indonesian Jurnal of Chemical Analysis, 2(2), 54-59.
  17. Chen. (2011). Optimization of Solvent-Free Microwave Extraction of Essential Oil from the Fruits of Schidndra chinenses and its DPPH Radical Scavenging Activity. Food Science, 32(14), 85-89.
  18. Delima, P.M. (2007). Peningkatan Kandungan Senyawa Oxygenated Terpen Pada Minyak Kemukus (Cubeb oil) dengan Pemisahan Menggunakan Pelarut. Institut Pertanian Bogor, Bogor.
  19. Lucchesi, M.E; Chemat, F; Smadja, J. (2016). Solvent-Free Microwave Extraction: An Innovative Tool for Rapid Extraction of Essential Oil From Aromatic Herbs and Spices. Journal of Microwave Power & electromagnetic Energy , 39(10), 3-4.
  20. Mohammad, R, Yayat, S dan Widyastiwi. (2019). Aktivitas Immunodulator Ekstrak Etanol Kemukus (Piper cubeba), Kiseureuh (Piper aduncum), dan Cabe Jawa (Piper retrofactum) pada Mencit Jantan Galur Balb/C. Jurnal Ilmu Kefarmasian Indonesia, 17 (2), 255 - 261.
  21. Suryani, Andi N, dan Syahrir. (2018). Optimasi Formula Gel Antioksidan Etanol Buah Bligo (Benencasahispida) dengan Metode Simplex Lattice Design (SLD), Jurnal Farmasi Galenika , 3 (2), 150-156.
  22. Noor, F, Indah, S dan Krisna, M. (2019). Produksi Minyak Atsiri Untuk Mengembangkan Desa Pelutan, Kecamatan Gebang, Purworejo, Sebagai Sentra Minyak Atsiri, Jurnal Abdimas Madani dan Lestari, 1 (2), 79-96
  23. Kusumarini, N. (2016). Keanekaragaman Kemukus di Jawa, Jurnal Program Studi Biologi Tumbuhan , 1 (1), 6-7
  24. Devinta, A, Juhari, Ayu C, K. (2019). Perbandingan Metode Microwave Assisten Distillation (MAD) dan Microwave Assisted Distillation (MAHD) terhadap jumlah yield dan Mutu Minyak Atsiri dari Kulit Jeruk Manis, Jurnal eUREKA, 3 (1), 1-11
  25. Emrizal dan Siti, S. (2018). Uji Aktivitas Antibakteri Ekstrak Etanol Buah Kemukus Terhadap Bakteri. Jurnal Penelitian Farmasi Indonesia, 6 (2), 72-80
  26. Megawati, Murniyawati, F. (2015). Microwave Assisted Hydro-distillation untuk Ekstraksi Minyak Atsiri dari Kulit Jeruk Bali sebagai Lilin Aromaterapi. Jurna Bahan Alam Terbarukan, 4 (1), 18-26